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2,4,6,8-Tetrakis(2-methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonan-9-one diethyl ether hemisolvate
Fun H.-K, Yeap C.S, Rajesh K, ,
Published in International Union of Crystallography (IUCr)
2009
Volume: 65
   
Issue: 10
Pages: o2486 - o2487
Abstract
In the title compound, C35H36N2O5·0.5C 4H10O, the asymmetric unit contains one bicyclo-[3.3.1]nonane mol-ecule and a half-occupancy diethyl ether solvent with the O atom lying on a crystallographic inversion center. Two intra-molecular N- H⋯O hydrogen bonds generate S(6) ring motifs. The bicyclo-[3.3.1]nonane ring system adopts a chair-boat conformation. In the crystal structure, the mol-ecules are linked by weak inter-molecular C- H⋯N hydro-gen bonds into chains along the b axis; additional stabilization is provide by C- H⋯π inter-actions.
About the journal
JournalActa Crystallographica Section E Structure Reports Online
PublisherInternational Union of Crystallography (IUCr)
ISSN16005368
Open AccessNo