The current research describes the synthesis and testing of FRP under tensile loading and high temperature conditions. The FRP is produced using Vacuum Infusion technique and cut in to different fibre sizes. The SEM (Scanning Electron Microscope) analysis is performed to determine the effect of matrix maturity, temperature, fibre inclination, and loading rate on fibre matrix. The findings have shown relationship of fibre volume on thermal and mechanical characteristics of FRP. © IAEME Publication Scopus Indexed.