This research article examines the metallurgical and mechanical behavior of twenty-first-century nickel-based superalloy 686. The weld joints were produced with ERNiCrMo-4 and ERNiCrMo-14 filler wires by continuous current gas tungsten arc welding (GTAW) and pulsed current gas tungsten arc welding (PCGTAW) mode. Optical and scanning electron microscope (SEM) analyses were performed to evaluate the microstructure of welded joints. PCGTAW weldments showed refined microstructure, narrower weld bead and minimum heat-affected zone compared to GTAW. SEM analysis revealed the presence of secondary phases in the interdendritic regions of GTA and PCGTA weldments made of ERNiCrMo-4 and GTA ERNiCrMo-14 fillers. Energy-dispersive X-ray spectroscopy examination was also performed to assess the microsegregation of alloying elements in the weldments. The results proved nonexistence of microsegregation in the case of PCGTA weldments made by ERNiCrMo-14 filler. However, segregation of alloying element Mo was noticed in other weldments. Strength and toughness of the weld joints were evaluated by conducting tensile and Charpy impact tests. The refined microstructure with the absence of microsegregation obtained in the PCGTA welding made with ERNiCrMo-14 filler wire resulted in the higher strength and toughness than other weldments. © 2018, The Indian Institute of Metals - IIM.

Manikandan M

Department of Design and Automation

School of Mechanical Engineering

Vellore Campus

Arulmurugan B

Vellore Institute of Technology (VIT) is a private university located in&nbsp;Tamil Nadu, India. Founded in 1984, as Vellore Engineering College, the institution offers 20 undergraduate, 34 postgraduate, four integrated and four research programs. It has campuses in Vellore, Amravati, Bhopal and Chennai.

VIT is one of the top ranked private universities in India according to NIRF, THE and QS Rankings.&nbsp;Govt. of India has recognized&nbsp;VIT, Vellore as an&nbsp;Institution of Eminence. This has allowed VIT to take independent quality initiatives and move up in world ranking.

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Transactions of the Indian Institute of Metals

In the present study, microstructure and the corrosion behavior of Nickel based superalloy 686 and its weld joints has been investigated by synthetic sea water environment. The weldments were fabricated by Gas Tungsten Arc Welding (GTAW) and Pulsed Current Gas Tungsten Arc Welding (PCGTAW) techniques with autogenous mode and three different filler wires (ERNiCrMo-4, ERNiCrMo-10 and ERNiCrMo-14). Microstructure and Scanning electron microscope examination was carried out to evaluate the structural changes in the fusion zones of different weldments. Energy Dispersive X-ray Spectroscopy (EDS) analysis was carried out to evaluate the microsegregation of alloying elements in the different weld joints. Potentiodynamic polarization study was experimented on the base metal and weld joints in the synthetic sea water environment to evaluate the corrosion rate. Tafel's interpolation technique was used to obtain the corrosion rate. The microstructure examination revealed that the fine equiaxed dendrites were observed in the pulsed current mode. EDS analysis shows the absence of microsegregation in the current pulsing technique. The corrosion rates of weldments are compared with the base metal. The results show that the fine microstructure with the absence of microsegregation in the PCGTA weldments shows improved corrosion resistance compared to the GTAW. Autogenous PCGTAW shows higher corrosion resistance irrespective of all weldments employed in the present study. © Published under licence by IOP Publishing Ltd.

Fulltext

IOP Conference Series: Materials Science and Engineering

Investigations on Microstructure and Corrosion behavior of Superalloy 686 weldments by Electrochemical Corrosion Technique

The present work investigates the microstructure and mechanical properties of alloy C-276 fabricated by continuous and pulsed current gas tungsten arc welding process and by employing ER2553 filler wire. Optical and scanning electron microscopic analyses were carried out to study the microstructures of weldments produced. Energy dispersive X-ray spectroscopy (EDS) was performed to investigate the formation of secondary phases in the weldments. The results disclosed that pulsed current gas tungsten arc welding showed refined microstructure compared to continuous current gas tungsten arc welding. SEM/EDS analysis revealed the segregation of Mo in the weld interface regions in both the welding techniques. The extent of microsegregation reduced the strength and toughness of the weld joint compared to the base metal. Bend test revealed cracks in the weld interface region in both the weldments. © 2017, The Indian Institute of Metals - IIM.

Analysis of Metallurgical and Mechanical Properties of Continuous and Pulsed Current Gas Tungsten Arc Welded Alloy C-276 with Duplex Stainless Steel

Superalloy C-276 is known to be prone to hot cracking during fusion welding by Gas Tungsten Arc method. Microsegregation occurring during cooling of fusion zone with consequent appearance of topologically close-packed phases P and l has been held responsible for the observed hot cracking. The present work investigated the possibility of suppressing the microsegregation in weldments by resorting to current pulse. Weldments were made by continuous current gas tungsten arc welding and pulsed current gas tungsten arc welding using ERNiCrMo-4 filler wire. The weld joints were studied with respect to microstructure, microsegregation, and mechanical properties. Optical microscopy and scanning electron microscopy were employed to study the microstructure. Energy-Dispersive X-ray Spectroscopy was carried out to evaluate the extent of microsegregation. Tensile testing was carried out to determine the strength and ductility. The results show that the joints fabricated with pulsed current gave rise to narrower welds with practically no heat affected zone, a refined microstructure in the fusion zone, reduced microsegregation, and superior combination of mechanical properties. © The Chinese Society for Metals and Springer-Verlag Berlin Heidelberg 2014.

Acta Metallurgica Sinica (English Letters)

Improvement of Microstructure and Mechanical Behavior of Gas Tungsten Arc Weldments of Alloy C-276 by Current Pulsing

In the present work, a Design Of Experiment (DOE) technique, the Taguchi method was employed to bead on welding trials to optimize Pulsed Current Gas Tungsten Arc (PCGTA) welding process parameters of alloy C-276. A L9 orthogonal array of Taguchi design involving nine experiments for four parameters (pulsed current, background current, % on time, pulse frequency) with three levels was used. An analysis of the mean of signal-to-noise (S/N) ratio indicates that the depth of current is influenced significantly by the levels in the Taguchi orthogonal array. The higher the better response category was selected to obtain optimum conditions for depth of penetration. The optimum conditions were found to be 165 A pulse current, 77 A background current, 60 % on time and 5 Hz pulse frequency. Analysis of Variance (ANOVA) is performed to measure percentage contribution of each factor. The results show that the pulse current was most influencing parameter on the depth of penetration and % on time (23.28 %) the next most influencing. Confirmation test was carried out to validate the results of Taguchi analysis; the result shows that there is good match between expected and predicted results. © 2014 The Authors.

Procedia Engineering

Optimization of the Pulsed Current Gas Tungsten Arc Welding Process Parameters for alloy C-276 using the Taguchi Method

Effects of switching over from gas tungsten arc welding (GTAW) to pulsed current gas tungsten arc welding (PCGTAW) on the quality of joints produced in Hastelloy C-276 material were investigated. Welding was carried out both by autogenous mode and using ERNiCrMo-3 filler wire. Microstructures of weld joints produced with and without current pulsing were studied using optical and scanning electron microscopy. Microsegregation occurring in GTAW and PCGTAW joints was investigated using energy dispersive X-ray spectroscopy (EDS). Strength and ductility of weld joints produced with and without pulsing were evaluated. The results show that pulsing results in refined microstructure, reduced microsegregation and improved strength of weld joints. Secondary phase(s) noticed in GTA weldments were found to be absent in PCGTA weldments. Autogenous PCGTA weldments were found to be the best in terms of: (i) freedom from microsegregation, (ii) strength and (iii) freedom from unwanted secondary phases. © 2014 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.

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ISSN	0972-2815
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