This article presents a simple in-house laboratory experiment method for the simultaneous estimation of principal thermal conductivity and specific heat capacity of an orthotropic composite with non-intrusive temperature measurement. The principle of method involves in symmetrical heating of two identical samples with a planar heater sandwiched in-between them and measuring the temperature of non-heated surface non-intrusively using IR camera. The forward problem that mimics the heat conduction from heater to sample and then to ambient is a 3-D transient conduction equation which is solved using finite volume method whereas inverse problem is solved using Levenberg-Marquardt algorithm. At first numerical estimations are carried out with synthetic temperature data to decide upon the parameters to be identified/fixed as well as to find optimal experimental variables. Then, using measured temperature response of the non-heated surface, the thermal properties of unidirectional fiber reinforced carbon composite are estimated. Induced bias errors in the estimated parameters because of error in the fixed parameters are also approximately quantified. The estimated transverse thermal conductivity is found to be 0.72 W/m K whereas the in-plane conductivities parallel and perpendicular to fiber are 5.43 W/m K, 0.64 W/m K respectively. Also, the estimated specific heat capacity is found to be 1044 J/kg K. A maximum deviation of 10% from the absolute Guarded Hot Plate measurement is found in the estimated thermal conductivity parallel to fiber. © 2018 Elsevier Ltd