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Synthesis and characterization of some phosphazenium chloride salts, [R3PNH2]+Cl- (R = phenyl, p-chlorophenyl and morpholino)
Published in
Volume: 41
Issue: 2
Pages: 147 - 149
Some phosphazenium chloride salts of the type [R3PNH 2]+Cl-, where R = phenyl, p-chlorophenyl and morpholino, were synthesized by the reaction of the corresponding phosphiniminocyclotrithiazene compounds (R3PNS3N 3) with diphenyldichlorosilane in acetonitrile. All the products were characterized by analytical and spectroscopic data. The single crystal X-ray structure of [Ph3PNH2]+Cl- was reinvestigated with one mole of water molecule in the crystal lattice, showing an intermolecular hydrogen bonding. © Taylor & Francis Group, LLC.
About the journal
JournalSynthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry
Open AccessNo