Zirconium Ferrite (ZrFe2O5) was prepared by coprecipitation method at temperature as low as 80°C. The prepared samples were calcined at different temperatures like 400°C and 800°C. Synthesized nanoparticles were characterized by using X-ray diffraction (XRD), Scanning Electron Microscope (SEM), vibrating sample magnetometer (VSM) and transmission electron microscopy (TEM). We found that the size of nanoparticles increased with the increase in calcinations temperature. TEM was used to characterize the microstructure of the samples and particle size determination, which exhibited the formation of spherical nanoparticles.