Revolutions in nanotechnology enabled the development of advanced nanocomposites with superior properties for engineering applications especially in automotive and aerospace industries. Among this carbonaceous nano materials like MWCNT have got more attention. Addition of MWCNT in metal matrix results in retardation of friction coefficient and improvement on other mechanical properties based on its dispersion. MWCNT won't have sufficient space to occupy over the powder surface, when the addition is beyond a limit and acts as a solid lubricant during milling. Investigations on self lubricating property during milling were done by using scanning electron microscope, X-ray diffraction and powder density. Uniform dispersion was the bottleneck to utilize their attractive properties of the reinforcement. An attempt had been done for a uniform dispersion during premixing process using a combination of ultra-sonication, magnetic and mechanical stirring followed by high energy ball milling. © 2019 Elsevier Ltd.